What substance is used in the industrial preparation of methyl diantilis to reduce the aldehyde group of 3-ethoxy-4-hydroxybenza
ldehyde?
1 answer:
Answer:
Sodium Borohydride (NaBH₄)
Explanation:
Methyl diantilis (2-Ethoxy-4-(methoxymethyl)phenol) is a fragrance compound which smells like Vanilla. This compound is being synthesized from 3-ethoxy-4-hydroxybenzaldehyde also known as Ethyl Vanillin in two steps.
Step 1: Reduction of Aldehydic Group on Ethyl Vanillin:
The benzaldehyde derivative is treated with a mild reducing agent i.e. NaBH₄ (Sodium Borohydride). NaBH₄ is a source of Hydride (H⁻) ion and undergoes nucleophilic substitution reaction yielding 2-ethoxy-4-(hydroxymethyl)phenol.
Step 2: Etherification of 2-ethoxy-4-(hydroxymethyl)phenol:
In the second step 2-ethoxy-4-(hydroxymethyl)phenol is treated with Methanol in the presence of strong acidic polymeric resin known as Amberlyst-15-wet resulting in the formation of Methyl diantilis as shown in attached figure.
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Answer : The grams of consumed is, 89.6 grams.
Solution : Given,
Mass of = 265 g
Molar mass of = 80 g/mole
Molar mass of = 28 g/mole
First we have to calculate the moles of .
The given balanced reaction is,
from the reaction, we conclude that
As, 1 mole of produces from 1 mole of
So, 3.2 moles of produces from 3.2 moles of
Now we have to calculate the mass of
Therefore, the grams of consumed is, 89.6 grams.